An article Suzuki coupling of aroyl-MIDA boronate esters – A preliminary report on scope and limitations WOS:000658811700009 published article about POTASSIUM ACYLTRIFLUOROBORATES KATS; N-C CLEAVAGE; ARYLBORONIC ACIDS; CARBOXYLIC ANHYDRIDES; CATALYZED SYNTHESIS; KETONE SYNTHESIS; ACYL CHLORIDES; ARYL KETONES; REAGENTS; AMIDES in [Lai, Samson; Takaesu, Noah; Lin, Wen Xuan; Perrin, David M.] Univ British Columbia, Chem Dept, 2036 Main Mall, Vancouver, BC V6T 1Z1, Canada in 2021.0, Cited 58.0. The Name is Benzophenone. Through research, I have a further understanding and discovery of 119-61-9. COA of Formula: C13H10O
Recent methodological reports for synthesizing acyl-MIDA boronate esters compel an investigation of their potential use as substrates in a standard Suzuki-Miyaura cross-coupling reaction. Here we report the production of benzophenones by C-C cross coupling between a benzoyl-MIDA boronate ester and a multitude of aryl bromide substrates in adequate yields following optimization under ambient conditions outside of a glove box. Under these standard conditions, none of several acyl-MIDA boronate esters (in an alkyl series) serves as a competent coupling partner. The substrate scope is also limited by the finding that the corresponding trifluoroborates of both acyl- and aroyltrifluroborates are not suitable substrates. For reasons of availability and synthetic difficulty in procuring other aroyl-MIDA boronates, this preliminary study examines the reactivity of benzoyl-MIDA boronate with several aryl bromide substrates. (C) 2021 Elsevier Ltd. All rights reserved.
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Reference:
Thiomorpholine – Wikipedia,
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