An article Development of an efficient, one-pot, multicomponent protocol for synthesis of 8-hydroxy-4-phenyl-1,2-dihydroquinoline derivatives WOS:000595020700001 published article about QUINOLINE DERIVATIVES; BIOLOGICAL EVALUATION; MALDI-TOF; DESIGN; ANTIBACTERIAL; CHLOROQUINE; CHEMISTRY; CATALYST; 8-HYDROXYQUINOLINE; DEHYDROGENATION in [Tabassum, Rukhsana; Ashfaq, Muhammad] Islamia Univ Bahawalpur, Dept Chem, Bahawalpur 36100, Pakistan; [Oku, Hiroyuki] Gunma Univ, Grad Sch Sci & Engn, Div Mol Sci, Gunma, Japan in 2021, Cited 93. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6. Safety of 3-Nitrobenzaldehyde
A one-pot quick and efficient multicomponent reaction has been developed for the synthesis of a new series of functionalized 8-hydroxy-4-phenyl-1,2-dihydroquinoline derivatives using 30 mol% ammonium acetate in ethanol as solvent. This economical protocol run smoothly to give variety of quinoline derivatives in 55% to 98% yield from inexpensive reagents and catalyst in mild reaction conditions. Various spectroscopic techniques like FTIR, H-1 NMR and C-13 NMR, MALDI-TOF-MS, and EI-MS were used to study and confirm their structure.
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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem