An article N-donor 2-(Sulfonamido)benzamide ligands, their palladium(II) coordination species and C-C coupling catalysis efficiencies WOS:000487932000035 published article about SUZUKI-MIYAURA REACTION; PRE-CATALYSTS; COMPLEXES; ARYL; CHLORIDES; NANOPARTICLES; IMIDAZOLE; NICKEL; SERIES in [Oloyede, Hammed Olawale; Woods, Joseph Anthony Orighomisan] Univ Ibadan, Dept Chem, Inorgan Chem Unit, Ibadan, Nigeria; [Oloyede, Hammed Olawale; Goerls, Helmar; Plass, Winfried; Eseola, Abiodun Omokehinde] Friedrich Schiller Univ Jena, Inst Anorgan & Analyt Chem, Humboldtstr 8, D-07743 Jena, Germany; [Eseola, Abiodun Omokehinde] Redeemers Univ Ede, Dept Chem Sci, Mat Chem Grp, Ede, Osun State, Nigeria in 2019, Cited 51. The Name is 2-Aminobenzamide. Through research, I have a further understanding and discovery of 88-68-6. Product Details of 88-68-6
A series of synthetically accessible ligands based on new 2-(R-sulfonamido)benzamide have been prepared (R = methyl for H3M; R = 4-toly for H3T and T2CN; R = 2,4,6-triisopropylphenyl for H(3)iP and HiPCN). The R-substituents were selected to vary in sizes. Allowing ligand H(3)iP and palladium acetate to stand in solvent leads to self-assembly of the well-defined solvent- and stoichiometry-controlled tetranuclear or hexanuclear coordination macromolecules Pd-4(iP)(2) and (PdHiP)(6), which were analysed by X-ray crystallography. It was observed that palladium active species for Suzuki coupling catalysis could be stabilized by these simple and synthetically assessable N-donor ligands as revealed by turnover frequencies reaching 5500h(-1). Electronic features of these N-donors appear to be more important than the steric properties. (C) 2019 Elsevier B.V. All rights reserved.
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