An article Oxidation/ MCR domino protocol for direct transformation of methyl benzene, alcohol, and nitro compounds to the corresponding tetrazole using a three-functional redox catalytic system bearing TEMPO/Co (III)-porphyrin/ Ni(II) complex WOS:000604627600001 published article about SCHIFF-BASE COMPLEX; HETEROGENEOUS CATALYST; REUSABLE CATALYST; GREEN SYNTHESIS; CHLOROPHYLL-A; EFFICIENT; REDUCTION; AMINES; POLYSALICYLALDEHYDE; NANOPARTICLES in [Mahmoudi, Boshra; Rostami, Amin] Univ Kurdistan, Coll Sci, Chem Dept, Pasdaran St, Sanandaj 6617715177, Iran; [Kazemnejadi, Milad] Univ Birjand, Coll Sci, Dept Chem, POB 97175-615, Birjand, Iran; [Hamah-Ameen, Baram Ahmed] Univ Sulaimani, Coll Sci, Chem Dept, Sulaymaniyah, Kurdistan Regio, Iraq in 2021, Cited 55. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6. Formula: C7H5NO3
A redox catalytic system for oxidation-reduction reactions and the domino preparation of tetrazole compounds from nitro and alcohol precursors was designed, prepared and characterized by UV-vis, GPC, TGA, XRD, EDX, XPS, VSM, FE-SEM, TEM, DLS, BET, NMR, and ICP analyses. The catalyst was prepared via several successive steps by demetalation of chlorophyll b, copolymerization with acrylated TEMPO monomers, complexation with Ni and Co metals (In two different steps), then immobilized on magnetic nanoparticles. The presence of three functional groups including TEMPO, coordinated cobalt, and coordinated nickel in the catalyst, allowed the oxidation of various types of alcohols, alkyl benzenes as well as the reduction of nitro compounds by a single catalyst. All reactions yielded up to 97 % selectivity for oxidation and reduction reactions. Next, the ability of the catalyst to successfully convert alcohol, methyl benzenes and nitro to their corresponding tetrazoles was studied.
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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem