Recently I am researching about ONE-POT SYNTHESIS; BIOLOGICAL EVALUATION; PROMOTED SYNTHESIS; DERIVATIVES; DESIGN; INHIBITORS; SCAFFOLD; BINDING; ACCESS, Saw an article supported by the Research Council of NorwayResearch Council of Norway [275043 CasCat]. Quality Control of 2-Aminobenzamide. Published in GEORG THIEME VERLAG KG in STUTTGART ,Authors: Elumalai, V; Hansen, JH. The CAS is 88-68-6. Through research, I have a further understanding and discovery of 2-Aminobenzamide
Herein is reported a substantially improved synthesis of 2-substituted benzimidazoles by condensation of 1,2-diaminoarenes and aldehydes using methanol as the reaction medium. The developed method afforded moderate to excellent yields (33-96%) at ambient temperature, displays high functional group tolerance, is conducted open to air, and requires only one minute reaction time under catalyst- and additive-free conditions. Moreover, the efficient protocol permits scale-up to multi-gram scale synthesis of benzimidazoles and will become a method of choice when constructing such heterocyclic systems.
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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem