Day: February 21, 2022

Authors Wu, ZH; He, ZC; Xu, YK; Wang, J; Lu, XH; Xia, QH; Zhou, D in SPRINGER published article about in [Wu, Zhonghan; He, Zhechao; Xu, Yinke; Wang, Jing; Lu, Xinhuan; Xia, Qinghua; Zhou, Dan] Hubei Univ, Minist Of Educ, Key Lab Synth & Applicat Organ Funct Mol, Wuhan 430062, Peoples R China in 2021.0, Cited 21.0. Application In Synthesis of 3-Nitrobenzaldehyde. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6

From the view of energy saving and environment protection, green catalysis has become one of the most important goals of chemists, including both the green preparation of catalyst and the highly efficient catalysis under mild reaction condition. Herein, N,N-dimethylaminopropyl-functionalized hybrid zeolite is firstly synthesized by one-step non-templating method, which is characterized by powder X-ray diffraction, Fourier-transform IR, thermogravimetric analysis, element analysis, scanning electron microscope, water contact angle measurements, inductively coupled plasma atomic emission spectrometry, and N-2 adsorption-desorption measurements. The functionalized hybrid zeolite can be directly used as base catalyst without any post modification and achieve high yields of corresponding products in the Knoevenagel condensation of benzaldehyde (or substituted benzaldehyde) with ethyl cyanoacetate at room temperature by using ethanol as solvent. By the comparison with other zeolite catalysts, the unique and excellent catalytic properties of N,N-dimethylaminopropyl-functionalized hybrid zeolite was ascribed to not only the synergic effect of basic property and hydrophobic/lipophilicity of the organic groups, but also the easier accessibility of bulky substrate molecules with highly exposed catalytic active sites over the solid catalyst. The recycling and control experiments show that it owes excellent reusable stability.

Application In Synthesis of 3-Nitrobenzaldehyde. Bye, fridends, I hope you can learn more about C7H5NO3, If you have any questions, you can browse other blog as well. See you lster.

Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Authors Xu, ZX; Su, LN; Chen, XF; Yang, Y in ROYAL SOC CHEMISTRY published article about AGGREGATION-INDUCED EMISSION; OPTICAL WAVE-GUIDE; RATIONAL DESIGN; SINGLE-CRYSTAL; TEMPERATURE; TETRAPHENYLETHYLENE; PHOTOLUMINESCENCE; FLUORESCENCE; CARBAZOLE; HYDROGEL in [Xu, Zixuan; Chen, Xiaofen; Yang, Ying] Lanzhou Univ, Coll Chem & Chem Engn, Key Lab Nonferrous Met Chem & Resources Utilizat, Lanzhou 730000, Gansu, Peoples R China; [Su, Linhan] 940th Hosp Joint Logist Support Force Chinese PLA, Lanzhou 730050, Gansu, Peoples R China in 2021.0, Cited 34.0. Recommanded Product: 119-61-9. The Name is Benzophenone. Through research, I have a further understanding and discovery of 119-61-9

A novel ionic liquid [TPE-Dim-DMe] (Br)(2) was successfully synthesiszed. With the change of temperature, quadruple transformations of structure were observed in the [TPE-Dim-DMe] (Br)(2) crystal, and it simultaneously displayed mechanochromic phenomena. In addition, its excellent solubility in water makes it a novel bioimaging agent.

Welcome to talk about 119-61-9, If you have any questions, you can contact Xu, ZX; Su, LN; Chen, XF; Yang, Y or send Email.. Recommanded Product: 119-61-9

Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

In 2019 J ORG CHEM published article about CROSS-COUPLING REACTION; TERMINAL ALKYNES; ETHYNYL BENZIODOXOLONES; CATALYZED ALKYNYLATION; SONOGASHIRA REACTIONS; ARENES; QUINAZOLINONE; AMIDATION; ACETYLENE; AMINATION in [Rohokale, Rajendra S.; Kalshetti, Rupali G.; Ramana, Chepuri V.] CSIR Natl Chem Lab, Div Organ Chem, Dr Homi Bhabha Rd, Pune 411008, Maharashtra, India; [Kalshetti, Rupali G.; Ramana, Chepuri V.] Acad Sci & Innovat Res, New Delhi 110025, India in 2019, Cited 80. The Name is 2-Aminobenzamide. Through research, I have a further understanding and discovery of 88-68-6. COA of Formula: C7H8N2O

The directed C-H alkynylation of 2-(hetero)arylquinazolin-4-ones has been explored with the ethynylbenziodoxolone reagent TIPS-EBX employing an Ir(III) catalyst. Complementary conditions for either monoalkynylation or dialkynylation have been developed. Also demonstrated is the broad scope of this reaction and the compatibility of various functional groups such as -F, -Cl, -Br, -CF3, -OMe, -NO2, and alkyl, etc.

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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Application In Synthesis of Benzophenone. Authors Sahin, MO; Sanli, O in ELSEVIER published article about in [Sahin, Merve Olukman] Hatay Mustafa Kemal Univ, Res & Applicat Ctr Technol & Res & Dev, Tayfur Sokmen Campus, Antakya, Hatay, Turkey; [Sanli, Oya] Gazi Univ, Fac Sci, Dept Chem, Ankara, Turkey in 2021.0, Cited 29.0. The Name is Benzophenone. Through research, I have a further understanding and discovery of 119-61-9

In this study, in-situ synthesis of zinc oxide (ZnO) nanoparticles was utilized as an effective approach to prepare poly(vinyl alcohol) (PVA) and poly(vinyl alcohol)-graft-acrylonitrile/2-hydroxyethyl methacrylate (PVA-g-AN/HEMA) membranes with ZnO nanoparticles. The membranes were characterized by using Frourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), differential scanning calorimetry (DSC), X-Ray diffraction (XRD) and contact angle measurements. Both of the membranes were utilized in separation of acetone/water mixtures via pervaporation technique and the optimum conditions regarding ZnO content within the membranes, acetone content in the feed solution and operating temperature were determined. PVA-g-AN/HEMA-ZnO nanocomposite membranes showed high permeation rate but low separation factor compared to PVA-ZnO nanocomposite membranes. Permeation rate and separation factor values were found to be in the range of 0.028-0.137 and 0.035-0.174 kg m(-2) h(-1), 17.61-325 and 9.4-84.5 depending on the pervaporation conditions for PVA-ZnO and PVA-g-AN/HEMA-ZnO nanocomposite membranes, respectively. (C) 2020 Elsevier B.V. All rights reserved.

Application In Synthesis of Benzophenone. Welcome to talk about 119-61-9, If you have any questions, you can contact Sahin, MO; Sanli, O or send Email.

Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Authors Gupta, R; Arora, G; Yadav, P; Dixit, R; Srivastava, A; Sharma, RK in ROYAL SOC CHEMISTRY published article about CATALYZED OXIDATIVE SYNTHESIS; ONE-POT SYNTHESIS; 4(3H)-QUINAZOLINONE DERIVATIVES; CASCADE SYNTHESIS; BENZYL ALCOHOLS; QUINAZOLINONES; METAL; EFFICIENT; SILICA; OXIDE in [Gupta, Radhika; Arora, Gunjan; Yadav, Priya; Dixit, Ranjana; Sharma, Rakesh Kumar] Univ Delhi, Green Chem Network Ctr, Dept Chem, Delhi 110007, India; [Yadav, Priya; Srivastava, Anju] Univ Delhi, Hindu Coll, Dept Chem, Delhi 110007, India in 2021, Cited 74. Name: 3-Nitrobenzaldehyde. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6

In the present work, we report the design and fabrication of a copper-containing ionic liquid supported magnetic nanocatalyst via a convenient and straightforward synthetic approach for the formation of 2-phenylquinazolin-4(3H)-ones using o-aminobenzamide and benzaldehydes as the reaction partners. The successful formation and properties of the as-prepared catalyst have been thoroughly investigated using diverse physico-chemical techniques including FT-IR, XRD, FE-SEM, TEM, ICP, VSM, BET and TGA. Using this nanocatalytic system, a variety of 2-phenylquinazolin-4(3H)-ones are synthesized in excellent yields with operational ease and short reaction times in an environmentally preferable solvent under open air and without using any external oxidizing agent. Besides, the catalyst possessed facile magnetic recoverability and remarkable reusability for six consecutive runs without any appreciable decrease in the catalytic efficiency.

Welcome to talk about 99-61-6, If you have any questions, you can contact Gupta, R; Arora, G; Yadav, P; Dixit, R; Srivastava, A; Sharma, RK or send Email.. Name: 3-Nitrobenzaldehyde

Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Application In Synthesis of 3-Nitrobenzaldehyde. Authors Gupta, S; Pathak, AK; Ameta, C; Punjabi, PB in BENTHAM SCIENCE PUBL LTD published article about in [Gupta, Sharoni; Ameta, Chetna; Punjabi, Pinki B.] Mohanlal Sukhadia Univ, Univ Coll Sci, Dept Chem, Microwave Synth Lab, Udaipur 313001, Rajasthan, India; [Pathak, Arpit K.] Shri Govind Guru Govt Coll, Dept Chem, Banswara 327001, Rajasthan, India in 2021.0, Cited 55.0. The Name is 3-Nitrobenzaldehyde. Through research, I have a further understanding and discovery of 99-61-6

An efficient, green and rapid protocol for one-pot synthesis of substituted imidazoles from isatin, aryl/hetero-aryl aldehydes and ammonium acetate in presence of CuO-TiO2-GO nanocomposite as catalyst under microwave irradiation has been reported in this article. The CuO-TiO2-GO nanocomposite was synthesized by the hydrothermal method. Further, the prepared composite was characterized by FT-IR, XRD, FESEM, EDS, TEM, Raman and TGA techniques. The protocol offered several advantages such as high rate of reaction, excellent yields, economic feasibility, simple work-up and reusability of catalyst up to six cycles. Further antimicrobial activities of the synthesized substituted imidazoles were evaluated by the broth dilution method.

Welcome to talk about 99-61-6, If you have any questions, you can contact Gupta, S; Pathak, AK; Ameta, C; Punjabi, PB or send Email.. Application In Synthesis of 3-Nitrobenzaldehyde

Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

Recently I am researching about HYDROGEN-PEROXIDE; C-H; POLYAZADENTATE COMPLEXES; SELECTIVE HYDROXYLATION; IRON(IV)-OXO COMPLEXES; EFFICIENT CATALYSTS; BENZOIC-ACIDS; OXIDATION; BENZENE; PHENOL, Saw an article supported by the Ministero dell’Universita e della RicercaMinistry of Education, Universities and Research (MIUR); Universita di Roma La Sapienza (Progetti di Ricerca 2018). Published in ROYAL SOC CHEMISTRY in CAMBRIDGE ,Authors: Ticconi, B; Capocasa, G; Cerrato, A; Di Stefano, S; Lapi, A; Marincioni, B; Olivo, G; Lanzalunga, O. The CAS is 90-44-8. Through research, I have a further understanding and discovery of Anthrone. Safety of Anthrone

The oxidation of a series of alkylaromatic compounds with H2O2 catalyzed by an imine-based non-heme iron complex prepared in situ by reaction of 2-picolylaldehyde, 2-picolylamine, and Fe(OTf)(2) in a 2 : 2 : 1 ratio leads to a marked chemoselectivity for aromatic ring hydroxylation over side-chain oxidation. This selectivity is herein investigated in detail. Side-chain/ring oxygenated product ratio was found to increase upon decreasing the bond dissociation energy (BDE) of the benzylic C-H bond in line with expectation. Evidence for competitive reactions leading either to aromatic hydroxylation via electrophilic aromatic substitution or side-chain oxidation via benzylic hydrogen atom abstraction, promoted by a metal-based oxidant, has been provided by kinetic isotope effect analysis.

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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

COA of Formula: C7H8N2O. Authors Thorve, PR; Maji, B in ROYAL SOC CHEMISTRY published article about in [Thorve, Pradip Ramdas; Maji, Biplab] Indian Inst Sci Educ & Res Kolkata, Dept Chem Sci, Mohanpur 741246, India in 2021, Cited 72. The Name is 2-Aminobenzamide. Through research, I have a further understanding and discovery of 88-68-6

Herein, we report a bioinspired catalytic system for the one-pot cascade oxidation of a native primary amine and an in situ generated non-native secondary amine. The catalyst consists of an o-quinone cofactor phd (1,10-phenanthroline-5,6-dione) and a copper ion and operates under ambient air conditions. Quinazolin-4(3H)-ones, which are common pharmacophores present in numerous pharmaceuticals and bioactive compounds, were synthesized in high yields. A detailed kinetic and mechanistic study elucidates the role of the catalyst in the multi-step oxidative cascade reaction.

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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

In 2019 ACTA CRYSTALLOGR C published article about ENANTIOSELECTIVE TOTAL-SYNTHESIS; ASYMMETRIC-SYNTHESIS; NATURAL-PRODUCTS; DERIVATIVES; ACID; CYCLOADDITION; QUINAZOLINONE; CONSTRUCTION; ANALOGS; SET in [Chernyshov, Vladimir V.; Gatilov, Yuri, V; Yarovaya, Olga, I; Koskin, Igor P.; Salakhutdinov, Nariman F.] NN Vorozhtsov Novosibirsk Inst Organ Chem SB RAS, 9 Acad Lavrentiev Ave, Novosibirsk 630090, Russia; [Chernyshov, Vladimir V.; Gatilov, Yuri, V; Yarovaya, Olga, I; Brylev, Konstantin A.] Novosibirsk State Univ, Pirogova St 2, Novosibirsk 630090, Russia; [Yarovoy, Spartak S.; Brylev, Konstantin A.] Nikolaey Inst Inorgan Chem SB RAS, 3 Acad Lavrentiev Ave, Novosibirsk 630090, Russia in 2019, Cited 41. The Name is 2-Aminobenzamide. Through research, I have a further understanding and discovery of 88-68-6. COA of Formula: C7H8N2O

The possibility of a single-stage solvent-free stereoselective synthesis of a spirocyclic compound from the natural bicyclic monoterpenoid (-)-fenchone and anthranilamide has been shown for the first time. The molecular and crystal structure of (1R,2S,4S)-1,3,3-trimethyl-10H-spiro[bicyclo[2.2.1]heptane-2,2′-quinazolin]-4′(3’H)-one, C17H22N2O, was established by X-ray diffraction though the chirality was assumed via the known reactant connectivity and H-1 and C-13 NMR spectroscopy. It has shown that in the molecule, for steric reasons, there is an elongation of the Me2C-C(N)N bond to 1.603 (5) A degrees. The formation of dimers via N-H center dot center dot center dot O C hydrogen bonds with an interaction energy of 93.30 kJ mol(-1) and through cavities (33.7% of the unit-cell volume) was established in the packing of the molecules. There are no pi-stacking interactions in the structure.

Welcome to talk about 88-68-6, If you have any questions, you can contact Chernyshov, VV; Gatilov, YV; Yarovaya, OI; Koskin, IP; Yarovoy, SS; Brylev, KA; Salakhutdinov, NF or send Email.. COA of Formula: C7H8N2O

Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem

An article Single-Crystal Cobalt Phosphide Nanorods as a High-Performance Catalyst for Reductive Amination of Carbonyl Compounds WOS:000651113700014 published article about NICKEL PHOSPHIDE; HYDROGEN EVOLUTION; PRIMARY AMINES; DOPED CARBON; CHEMOSELECTIVE HYDROGENATION; SELECTIVE HYDROGENATION; MOLECULAR-HYDROGEN; GENERAL-SYNTHESIS; NANOPARTICLES; EFFICIENT in [Sheng, Min; Fujita, Shu; Yamaguchi, Sho; Mizugaki, Tomoo; Mitsudome, Takato] Osaka Univ, Grad Sch Engn Sci, Dept Mat Engn Sci, Osaka 5608531, Japan; [Yamasaki, Jun] Osaka Univ, Res Ctr Ultrahigh Voltage Electron Microscopy, Ibaraki, Osaka 5670047, Japan; [Nakajima, Kiyotaka] Hokkaido Univ, Inst Catalysis, Sapporo, Hokkaido 0010021, Japan; [Yamazoe, Seiji] Tokyo Metropolitan Univ, Dept Chem, Tokyo 1920397, Japan; [Mizugaki, Tomoo] Osaka Univ, Innovat Catalysis Sci Div, Inst Open & Transdisciplinary Res Initiat ICS OTR, Suita, Osaka 5650871, Japan in 2021.0, Cited 50.0. The Name is Benzophenone. Through research, I have a further understanding and discovery of 119-61-9. SDS of cas: 119-61-9

The development of metal phosphide catalysts for organic synthesis is still in its early stages. Herein, we report the successful synthesis of single-crystal cobalt phosphide nanorods (Co2P NRs) containing coordinatively unsaturated Co-Co active sites, which serve as a new class of air-stable, highly active, and reusable heterogeneous catalysts for the reductive amination of carbonyl compounds. The Co2P NR catalyst showed high activity for the transformation of a broad range of carbonyl compounds to their corresponding primary amines using an aqueous ammonia solution or ammonium acetate as a green amination reagent at 1 bar of H-2 pressure; these conditions are far milder than previously reported. The air stability and high activity of the Co2P NRs is noteworthy, as conventional Co catalysts are air-sensitive (pyrophorous) and show no activity for this transformation under mild conditions. P-alloying is therefore of considerable importance for nanoengineering air-stable and highly active non-noble-metal catalysts for organic synthesis.

SDS of cas: 119-61-9. Welcome to talk about 119-61-9, If you have any questions, you can contact Sheng, M; Fujita, S; Yamaguchi, S; Yamasaki, J; Nakajima, K; Yamazoe, S; Mizugaki, T; Mitsudome, T or send Email.

Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem