Analyzing the synthesis route of 616-14-8

I hope my short article helps more people learn about this compound(1-Iodo-2-methylbutane)Synthetic Route of C5H11I. Apart from the compound(616-14-8), you can read my other articles to know other related compounds.

The chemical properties of alicyclic heterocycles are similar to those of the corresponding chain compounds. Compound: 1-Iodo-2-methylbutane, is researched, Molecular C5H11I, CAS is 616-14-8, about Synthetic methods and reactions. XIII. Preparation of alkyl halides from alcohols with alkali halides in polyhydrogen fluoride/pyridine solution, the main research direction is halide alkyl cycloalkyl adamantyl; benzyl halide; norbornyl halide.Synthetic Route of C5H11I.

Thirty-nine RX (R = C4-8 alkyl, cyclopentyl, cyclohexyl, adamantyl, norbornyl, PhCH2; X = F, Cl, Br, I) were prepared by reaction of the corresponding ROH with MX (M = Na, K, NH4) in polyhydrogen fluoridepyridine. Thus, BuCH2OH was kept 1 hr with 70% HF-pyridine containing NaCl to give 89% BuCH2Cl.

I hope my short article helps more people learn about this compound(1-Iodo-2-methylbutane)Synthetic Route of C5H11I. Apart from the compound(616-14-8), you can read my other articles to know other related compounds.

Reference:
Thiomorpholine – Wikipedia,
Thiomorpholine | C4H9NS – PubChem