An article Ti-superoxide catalyzed oxidative amidation of aldehydes with saccharin as nitrogen source: synthesis of primary amides WOS:000507289600012 published article about SOLVENT-FREE CONDITIONS; RHINOVIRUS 3C PROTEASE; STRUCTURE-BASED DESIGN; ONE-POT SYNTHESIS; HETEROGENEOUS CATALYST; TITANIUM SUPEROXIDE; CARBOXYLIC-ACIDS; PRIMARY AMINES; ALCOHOLS; AMMONIA in [Kamble, Rohit B.; Mane, Kishor D.; Rupanawar, Bapurao D.; Sudalai, A.; Suryavanshi, Gurunath] CSIR, Natl Chem Lab, Chem Engn & Proc Dev Div, Pune 411008, Maharashtra, India; [Kamble, Rohit B.; Mane, Kishor D.; Rupanawar, Bapurao D.; Sudalai, A.; Suryavanshi, Gurunath] Acad Sci & Innovat Res, Ghaziabad 201002, UP, India; [Korekar, Pranjal] MES Abasaheb Garware Coll, Dept Chem, Pune 411004, Maharashtra, India in 2020, Cited 55. The Name is 2-Aminobenzamide. Through research, I have a further understanding and discovery of 88-68-6. Recommanded Product: 2-Aminobenzamide
A new heterogeneous catalytic system (Ti-superoxide/saccharin/TBHP) has been developed that efficiently catalyzes oxidative amidation of aldehydes to produce various primary amides. The protocol employs saccharin as amine source and was found to tolerate a wide range of substrates with different functional groups. Moderate to excellent yields, catalyst reusability and operational simplicity are the main highlights. A possible mechanism and the role of the catalyst in oxidative amidation have also been discussed.
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