Application In Synthesis of 2-Aminobenzamide. In 2020 ORG LETT published article about CATALYZED 3-COMPONENT REACTION; EFFICIENT SYNTHESIS; FACILE SYNTHESIS; ISOCYANATES; CYCLIZATION; CYCLOADDITION; DERIVATIVES; CHEMISTRY; INSERTION; CHLORIDE in [Malviya, Bhanwar Kumar; Sharma, Siddharth] Mohanlal Sukhadia Univ, Dept Chem, Udaipur 313001, Rajasthan, India; [Jaiswal, Pradeep K.] Texas A&M Univ, Dept Biochem & Biophys, College Stn, TX 77843 USA; [Verma, Ved Prakash] Banasthali Univ, Dept Chem, Vanasthali 304022, India; [Badsara, Satpal Singh] Rajasthan Univ, Dept Chem, Jaipur 302004, Rajasthan, India in 2020, Cited 85. The Name is 2-Aminobenzamide. Through research, I have a further understanding and discovery of 88-68-6.
This work discloses an electrochemical oxidative cross-coupling of amines with aryl and aliphatic isocyanides. In an undivided cell, the reaction proceeds without involving any transition-metal catalyst, oxidant, or toxic reagents providing carbodiimides in good yields, thereby circumventing stoichiometric chemical oxidants, with H-2 as the only byproduct. Moreover, carbodiimides were in situ converted into unsymmetrical ureas in moderate to good yields using an electricity ON-OFF strategy.
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Reference:
Thiomorpholine – Wikipedia,
,Thiomorpholine | C4H9NS – PubChem